(E)-1-甲基-1,2二苯基乙烯合成路线 (共 175 条)
反应条件
triethylamine in N,N-dimethyl-formamide T=100°C; Heck reaction; 18 h;
参考文献
Heshmatpour, Felora; Abazari, Reza; Balalaie, Saeed
Tetrahedron, 2012 , vol. 68, # 14 p. 3001 - 3011
反应条件
sodium acetate in PEG-400; water T=80°C; Heck reaction; 24 h; Atmospheric conditions;
参考文献
Wu, Shang; Ma, Hengchang; Jia, Xiaojie; Zhong, Yunmei; Lei, Ziqiang
Tetrahedron, 2011 , vol. 67, # 1 p. 250 - 256
反应条件
palladium diacetate in N,N-dimethyl-formamide T=130°C; 0.0333333 h; Schlenk techniqueMicrowave irradiation; regioselective reaction;
参考文献
Li, Jian; Liu, Li; Ding, Dong; Sun, Jiang-Tao
Letters in Organic Chemistry, 2013 , vol. 10, # 1 p. 42 - 46
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2; tris-[3-carboxyphenyl]phosphine in water; toluene T=100°C; 2.5 h;
参考文献
Genin, Emilie; Michelet, Veronique; Genet, Jean-Pierre
Tetrahedron Letters, 2004 , vol. 45, # 21 p. 4157 - 4161
反应条件
chloro-trimethyl-silane; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; 8 h;
参考文献
Wang, Jin-Xian; Wang, Kehu; Zhao, Lianbiao; Li, Hongxia; Fu, Ying; Hu, Yulai
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 10-11 p. 1262 - 1270
反应条件
oxygen; palladium diacetate; sodium carbonate in acetonitrile T=50°C; 3 h;
参考文献
Jung, Young Chun; Mishra, Rajesh Kumar; Yoon, Cheol Hwan; Jung, Kyung Woon
Organic Letters, 2003 , vol. 5, # 13 p. 2231 - 2234
反应条件
oxygen; bis[2-(diphenylphosphino)phenyl] ether; palladium dichloride in methoxybenzene T=85°C; Heck type reaction; P=760.051 Torr; 24 h; optical yield given as percent de;
参考文献
Zhou, Xianya; Luo, Jiaying; Liu, Jing; Peng, Shengming; Deng, Guo-Jun
Organic Letters, 2011 , vol. 13, # 6 p. 1432 - 1435
反应条件
oxygen; palladium diacetate; sodium carbonate in acetonitrile T=50°C; 3 h; Title compound not separated from byproducts;
参考文献
Organic Letters, , vol. 5, # 13 p. 2231 - 2234
反应条件
1: meso-1,2-diphenylethylene With N,N,N',N'',N''-pentamethyldiethylenetriamine; sec.-butyllithium in tetrahydrofuran T=-25°C; 2 h; 2: methyl iodide in tetrahydrofuran T=-25 - 20°C; Further stages.;
参考文献
Cotter, Juliet; Hogan, Anne-Marie L.; O'Shea, Donal F.
Organic Letters, 2007 , vol. 9, # 8 p. 1493 - 1496
反应条件
NiCl2(PPh3)2 in tetrahydrofuran T=20°C; 12 h; Inert atmosphere;
参考文献
Yang, Zhaozhen; Chen, Xiaoyi; Kong, Wei; Xia, Siyuan; Zheng, Renwei; Luo, Fang; Zhu, Gangguo
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 13 p. 2175 - 2185