3,4,5-三甲氧苯乙胺盐酸盐合成路线 （共 5 条）
反应条件
1: With palladium on activated charcoal; hydrogen in methanol; chloroform 24 h; 2: With hydrogenchloride in methanol; diethyl ether; water
参考文献
Aksu, Kadir; Nar, Meryem; Tanc, Muhammet; Vullo, Daniela; Guelcin, Ilhami; Goeksu, Sueleyman; Tuemer, Ferhan; Supuran, Claudiu T.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 11 p. 2925 - 2931
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran 5 h; Cooling with iceReflux; 2: With hydrogenchloride in diethyl ether
参考文献
Zheng, Can-Hui; Chen, Jun; Liu, Jia; Zhou, Xiao-Tian; Liu, Na; Shi, Duo; Huang, Jing-Jing; Lv, Jia-Guo; Zhu, Ju; Zhou, You-Jun
Archiv der Pharmazie, 2012 , vol. 345, # 6 p. 454 - 462
反应条件
1.1: triethylamine; diphenyl phosphoryl azide / benzene 1.2: 30 h / 80 °C 2.1: hydrogen; palladium on activated charcoal / methanol; chloroform / 24 h View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 11 p. 2925 - 2931
反应条件
sulfuric acid; sodium nitrite T=50°C;
参考文献
Slotta; Mueller
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1936 , vol. 238, p. 14,22
反应条件
sodium hydroxide in methanol T=20°C; 3 h;
参考文献
Aksu, Kadir; Nar, Meryem; Tanc, Muhammet; Vullo, Daniela; Guelcin, Ilhami; Goeksu, Sueleyman; Tuemer, Ferhan; Supuran, Claudiu T.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 11 p. 2925 - 2931
