2,3,4,5,6-五氟苯磺酰氯合成路线 （共 32 条）
反应条件
chlorosulfonic acid T=120 - 130°C; 16 h;
参考文献
Horner, Leopold; Schmitt, Rolf-Erhard
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 189 - 212
反应条件
sulfuryl dichloride in tetrahydrofuran; hexane 3 h; Ambient temperature;
参考文献
Chen, Qing-Yun; Chen, Ming-Fang
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 7 p. 1071 - 1075
反应条件
in acetic acid 80percent H2O2, 0°C, 30 min;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
1: Mg / tetrahydrofuran / -20 - -10 °C 2: 52 percent / SO2Cl2 / hexane; tetrahydrofuran / 3 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1071 - 1075
反应条件
80percent H2O2, Cl2 steam for 2 h;
参考文献
Journal of the Chemical Society, , p. 3692 - 3703
反应条件
bis(benzonitrile)palladium(II) dichloride; 2,6-di-tert-butyl-pyridine T=140°C; 4 h;
参考文献
Kamigata, Nobumasa; Yoshikawa, Manabu; Shimizu, Toshio
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 134-135, p. 11 - 20
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
参考文献
Fei, Xiangshu; Zheng, Qi-Huang; Wang, Ji-Quan; Stone, K. Lee; Martinez, Tanya D.; Miller, Kathy D.; Sledge, George W.; Hutchins, Gary D.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 5 p. 1247 - 1251
反应条件
dichlorotris(triphenylphosphine)ruthenium(II) T=240°C; 0.25 h;
参考文献
Kamigata, Nobumasa; Yoshikawa, Manabu; Shimizu, Toshio
Journal of Fluorine Chemistry, 1998 , vol. 87, # 1 p. 91 - 95
反应条件
hexamethyl-silane; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylbenzene T=140°C; 3 h;
参考文献
Kashiwabara, Taigo; Tanaka, Masato
Tetrahedron Letters, 2005 , vol. 46, # 42 p. 7125 - 7128
