1-(苯基甲氧基)-3-(2-丙烯-1-基氧基)-2-丙醇合成路线 （共 9 条）
反应条件
1: 8 percent / I2; NaHCO3 / H2O; diethyl ether / 3 h / 0 °C 2: 63 percent / 18-crown-6 / dimethylformamide / 24 h / 80 °C View Scheme
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
iodine; sodium hydrogencarbonate in diethyl ether; water T=0°C; 3 h;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
N-iodo-succinimide in acetonitrile T=20°C;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
N-iodo-succinimide in acetonitrile 3 h; Heating;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
tris(pentafluorophenyl)-borane in dichloromethane
T=20°C; 4 h;
参考文献
Chandrasekhar; Raji Reddy; Nagendra Babu; Chandrashekar
Tetrahedron Letters, 2002 , vol. 43, # 21 p. 3801 - 3803
反应条件
sodium hydride
T=20°C; 4 h;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=25°C;
参考文献
Kose, Aytekin; Altundas, Ramazan; Secen, Hasan; Kara, Yunus
Helvetica Chimica Acta, 2013 , vol. 96, # 7 p. 1325 - 1330
反应条件
sodium hydroxide; tetra-n-butyl-ammonium sulfate in dichloromethane
Heating;
参考文献
Holmberg, Lars; Lindberg, Bengt; Lindqvist, Bengt
Carbohydrate Research, 1995 , vol. 268, # 1 p. 47 - 56
反应条件
1: 8 percent / I2; NaHCO3 / H2O; diethyl ether / 3 h / 0 °C
2: 63 percent / 18-crown-6 / dimethylformamide / 24 h / 80 °C
3: 90 percent / HCl / methanol / 20 °C
View Scheme
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
