2-羟基-1,4-萘醌合成路线 (共 313 条)
反应条件
1: 89 percent / SnCl2*2H2O, NaBH4 / ethanol / 0.5 h / 65 °C 2: 89 percent / Raney nickel / methanol / 20 h / Heating 3: H2SO4 / 0.25 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2233 - 2242
反应条件
hydrogenchloride; sodium hydroxide 1.) 60 deg C, 8 h, 2.) 80 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 58, # 4 p. 840 - 843
反应条件
in toluene 12 h; Var.: Aliquat 336 instead of 18-Crown-6;
参考文献
Tetrahedron Letters, , vol. 25, # 21 p. 2213 - 2214
反应条件
ethanol; sulfuric acid
参考文献
Chemische Berichte, , vol. 14, p. 1900
反应条件
acetic acid T=140 - 150°C;
参考文献
Chemische Berichte, , vol. 14, p. 1494
参考文献
Asahi; Tanaka; Shinozaki
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 8 p. 3093 - 3099
反应条件
hydrogenchloride Heating;
参考文献
Molecules, , vol. 5, # 3 p. 508 - 509
参考文献
Justus Liebigs Annalen der Chemie, , vol. 134, p. 377
反应条件
water in ethanol T=70°C; μ=0.5, var. pH and temp.; mechanism, Ea; Rate constantKineticsThermodynamic data;
参考文献
Journal of Pharmaceutical Sciences, , vol. 80, # 6 p. 573 - 577
反应条件
hydrogenchloride; KCl buffer; sodium chloride in ethanol T=70°C; E(activ.); other temperatures, other buffers: effect of pH, no influence of ionic strength; Product distributionKineticsThermodynamic data;
参考文献
Journal of Pharmaceutical Sciences, , vol. 83, # 3 p. 336 - 338