2,5-二甲基-1-苯基吡咯-3-羰醛合成路线 （共 8 条）
反应条件
trichlorophosphate
T=110°C; 6 h;
参考文献
Mao, Yongjun; Lin, Nan; Tian, Wang; Huang, Ziwei; An, Jing
Heterocycles, 2012 , vol. 85, # 5 p. 1179 - 1185
反应条件
1: With N,N-dimethyl-formamide; trichlorophosphate in toluene
T=80°C; 3 h;
2: With water; sodium carbonate in toluene
T=20°C; Product distribution / selectivity;
参考文献
REGENTS OF THE UNIVERSITY OF CALIFORNIA
Patent: US2008/293766 A1, 2008 ;
Location in patent: Page/Page column 10 ;
反应条件
diethyl ether; trichlorophosphate
参考文献
Brooker et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1875,1877
Journal of the American Chemical Society, 1951 , vol. 73, p. 5332,5337
反应条件
1: aminosulfonic acid / 3 h / 20 °C
2: trichlorophosphate / 3 h / 0 - 60 °C
View Scheme
参考文献
Urbano, Mariangela; Guerrero, Miguel; Velaparthi, Subash; Crisp, Melissa; Chase, Peter; Hodder, Peter; Schaeffer, Marie-Therese; Brown, Steven; Rosen, Hugh; Roberts, Edward
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 22 p. 6739 - 6745
反应条件
toluene; trichlorophosphate
参考文献
Rips; Buu-Hoi
Journal of Organic Chemistry, 1959 , vol. 24, p. 372
反应条件
toluene; trichlorophosphate
anschliessenden Behandeln mit Natriumacetat in Wasser;
参考文献
Rips; Buu-Hoi
Journal of Organic Chemistry, 1959 , vol. 24, p. 372
反应条件
1: aminosulfonic acid / 3 h / 20 °C
2: trichlorophosphate / 3 h / 0 - 60 °C
View Scheme
参考文献
Urbano, Mariangela; Guerrero, Miguel; Velaparthi, Subash; Crisp, Melissa; Chase, Peter; Hodder, Peter; Schaeffer, Marie-Therese; Brown, Steven; Rosen, Hugh; Roberts, Edward
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 22 p. 6739 - 6745
反应条件
formic acid; hydroxylamine hydrochloride
0.5 h; Heating;
参考文献
Jarvest; Marshall
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 6 p. 1401 - 1403
