反应条件
1: 1.) n-BuLi / 1.) THF, -78 to 0 deg C; 2.) -110 deg C to r.t., 2 h
2: 1.) 9-BBN; 2.) 3 M NaOH, 30 percent H2O2 / 1.) 2h, r.t., THF; 2.) reflux, 1.5 h
3: 90 percent / acetonitrile / 0.5 h / Ambient temperature
View Scheme
参考文献
Soderquist, John A.; Anderson, Charles L.
Tetrahedron Letters, 1988 , vol. 29, # 23 p. 2777 - 2778
