2,3-二甲基-5-甲氧基吲哚合成路线 （共 24 条）
反应条件
in acetic acid
1.5 h; Heating;
参考文献
Takemoto, Masumi; Iwakiri, Yasutaka; Tanaka, Kiyoshi
Heterocycles, 2007 , vol. 72, p. 373 - 383
反应条件
[Ru(CO)2(4,5-bis(diphenylphosphino)-9,9-dimethyl-9H-xanthene)]2; [Ru(CO)2(4,5-bis(diphenylphosphino)-9,9-dimethyl-9H-xanthene)]2; toluene-4-sulfonic acid in 1,1-dimethylpropan-1-ol
T=120°C; regioselective reaction;
参考文献
Zhang, Min; Xie, Feng; Wang, Xiaoting; Yan, Fengxia; Wang, Ting; Chen, Mengmeng; Ding, Yuqiang
RSC Advances, 2013 , vol. 3, # 17 p. 6022 - 6029
反应条件
FeBr2 in toluene
T=140°C; 16 h; Schlenk techniqueInert atmosphere;
参考文献
Nguyen, Quyen; Nguyen, Tuyen; Driver, Tom G.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 620 - 623
反应条件
tri-ruthenium(0)dodecacarbonyl; p-methoxyphenylammonium chloride
T=140°C;
参考文献
Tokunaga, Makoto; Ota, Mitsuru; Haga, Masa-aki; Wakatsuki, Yasuo
Tetrahedron Letters, 2001 , vol. 42, # 23 p. 3865 - 3868
反应条件
toluene-4-sulfonic acid in ethanol
Fischer cyclization; 1 h; Heating;
参考文献
Lim, Young-Kwan; Cho, Cheon-Gyu
Tetrahedron Letters, 2004 , vol. 45, # 9 p. 1857 - 1859
反应条件
pyridine
T=125°C; 2 h; Microwave irradiationInert atmosphere;
参考文献
Zhang, Jinzhu; Yin, Zhiwei; Leonard, Patrick; Wu, Jing; Sioson, Kate; Liu, Che; Lapo, Robert; Zheng, Shengping
Angewandte Chemie - International Edition, 2013 , vol. 52, # 6 p. 1753 - 1757
Angew. Chem., 2013 , vol. 125, # 6 p. 1797 - 1801,5
反应条件
FeBr2 in toluene
T=140°C; 12 h; Inert atmosphereSchlenk technique; Reagent/catalyst;
参考文献
Nguyen, Quyen; Nguyen, Tuyen; Driver, Tom G.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 620 - 623
反应条件
1: sec.-butyllithium With zinc dibromide in tetrahydrofuran; hexane
T=0°C; 0.166667 h; Inert atmosphere;
2: 4-methoxybenzenediazonium tetrafluoroborate With zinc dibromide in tetrahydrofuran
T=-60 - 25°C; Inert atmosphere;
3: in tetrahydrofuran
T=125°C; 2 h; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Haag, Benjamin A.; Zhang, Zhi-Guang; Li, Jin-Shan; Knochel, Paul
Angewandte Chemie - International Edition, 2010 , vol. 49, # 49 p. 9513 - 9516
反应条件
FeBr2 in toluene
T=140°C; 24 h; Inert atmosphereSchlenk technique;
参考文献
Nguyen, Quyen; Nguyen, Tuyen; Driver, Tom G.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 620 - 623
反应条件
RhH(CO)(triphenylphosphine)3; hexafluoroisopropyl alcohol
Inert atmosphereReflux;
参考文献
Saito, Akio; Oda, Shoko; Fukaya, Haruhiko; Hanzawa, Yuji
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1517 - 1524
