DL-3-苯基-2-羟丙酸合成路线 （共 84 条）
反应条件
bei 10-stdg. Erhitzen;
参考文献
Acta Academiae Aboensis, Series B: Mathematica et Physica, , vol. 10, # 14 p. 13,36
Chem. Zentralbl., , vol. 108, # II p. 1818
参考文献
Chemische Berichte, , vol. 63, p. 2765,2774
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 62, p. 1697,1710
反应条件
bei 0.5-stdg. Erhitzen;
参考文献
Acta Academiae Aboensis, Series B: Mathematica et Physica, , vol. 12, # 5 p. 6,20
Chem.Abstr., , p. 2413
Chem. Zentralbl., , vol. 113, # II p. 1122
反应条件
1: K2CO3 / acetone / 1.) room temperature, 1 h, 2.) reflux, overnight 2: 1.) Tf2O, 2,6-lutidine / 1.) CH2Cl2, 0 deg C, 15 min, 2.) room temperature, 2 h View Scheme
参考文献
Hoffman, Robert V.; Tao, Junhua
Journal of Organic Chemistry, 1997 , vol. 62, # 7 p. 2292 - 2297
反应条件
Lactobacillus paracasei DSM 20207 in water T=42°C; pH=6; 24 h; Product distribution; Further Variations:Reagents;
参考文献
Bodlenner, Anne; Glueck, Silvia M.; Nestl, Bettina M.; Gruber, Christian C.; Baudendistel, Nina; Hauer, Bernhard; Kroutil, Wolfgang; Faber, Kurt
Tetrahedron, 2009 , vol. 65, # 36 p. 7752 - 7755
反应条件
1: Pseudomonas sp. lipase Amano PS-C-II / diisopropyl ether / 48 h / 25 °C 2: bis-Tris buffer; MgCl2; Lactobacillus paracasei DSM 20008 / 42 °C / pH 6.5 View Scheme
参考文献
Larissegger-Schnell, Barbara; Glueck, Silvia M.; Kroutil, Wolfgang; Faber, Kurt
Tetrahedron, 2006 , vol. 62, # 12 p. 2912 - 2916
反应条件
cellulose-modified silica gel in hexane; isopropyl alcohol Resolution of racemate;
参考文献
Bai, Lian-Yang; Zhang, Yu-Ping; Deng, Pu-Hong; Zhang, Yi-Jun; Chen, Jun
Asian Journal of Chemistry, 2012 , vol. 24, # 11 p. 4917 - 4922
参考文献
Biquard
Annales de Chimie (Cachan, France), 1933 , vol. <10> 20, p. 97,113
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Khumtaveeporn, Kanjai; Ullmann, Astrid; Matsumoto, Kazutsugu; Davis, Benjamin G.; Jones
Tetrahedron Asymmetry, 2001 , vol. 12, # 2 p. 249 - 261
反应条件
caesium carbonate 1) MeOH, water, 2) DMF, a) 2 h, ice-bath, b) r.t., overnight; Yield given. Multistep reaction;
参考文献
Uesusuki, Shinya; Watanabe, Bunta; Yamamoto, Shuji; Otsuki, Junko; Nakagawa, Yoshiaki; Miyagawa, Hisashi
Bioscience, Biotechnology and Biochemistry, 2004 , vol. 68, # 5 p. 1097 - 1105
