DL-3-苯基-2-羟丙酸合成路线 （共 84 条）
反应条件
hydrogenchloride; sodium nitrite
参考文献
Biochemical Journal, , vol. 65, p. 651,657
反应条件
sodium nitrite in sulfuric acid; water; ethyl acetate; Petroleum ether
参考文献
Societe Civile Bioprojet
Patent: US5599951 A1, 1997 ;
反应条件
potassium hydroxide in methanol T=20°C; 12 h; Inert atmosphere;
参考文献
Concellon, Jose M.; Bernad, Pablo L.; Rodriguez-Solla, Humberto; Diaz, Pamela
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 13 p. 2178 - 2184
反应条件
1.) hydrochloric acid, methanol, 0-20 deg C, 12h; 2.) reflux, 1h; Yield given. Multistep reaction;
参考文献
Canadian Journal of Chemistry, , vol. 67, # 6 p. 1065 - 1070
反应条件
4-NH2-TEMPO-immobilized poly(p-phenylene benzobisthiazole); sodium hydrogencarbonate; sodium bromide in water; acetonitrile T=0°C; Electrolysis;
参考文献
Kubota, Jun; Ido, Toru; Kuroboshi, Manabu; Tanaka, Hideo; Uchida, Tetsuya; Shimamura, Kaoru
Tetrahedron, 2006 , vol. 62, # 20 p. 4769 - 4773
反应条件
hydrogenchloride; mercury; zinc in toluene T=100°C; 6 h;
参考文献
Wong; Xu; Chang; Lee
Synthesis, 1992 , # 8 p. 793 - 797
反应条件
[Ir(III)Cp*(bpy)(OH2)](SO4); ammonium formate in water T=80°C; pH=5.0; 6 h;
参考文献
Journal of the American Chemical Society, , vol. 126, # 10 p. 3020 - 3021
反应条件
formic acid; Ru2(cod)2(OCOCF3)4-1,4-bis(diphenylphosphino)butane; triethylamine; 1,4-di(diphenylphosphino)-butane in 1,4-dioxane 4 h; Heating;
参考文献
Maruyama, Yooichiroh; Sezaki, Takao; Tekawa, Masafumi; Sakamoto, Toshiaki; Shimizu, Isao; Yamamoto, Akio
Journal of Organometallic Chemistry, 1994 , vol. 473, # 1-2 p. 257 - 264
反应条件
zinc dibromide in dichloromethane Reduction;
参考文献
Javier Aladro; Guerra, Francisco M.; Javier Moreno-Dorado; Bustamante, Jesus M.; Jorge, Zacarias D.; Massanet, Guillermo M.
Tetrahedron Letters, 2000 , vol. 41, # 17 p. 3209 - 3213
反应条件
sodium methylate T=20°C; 24 h;
参考文献
Kreye, Oliver; Westermann, Bernhard; Wessjohann, Ludger A.
Synlett, 2007 , # 20 p. 3188 - 3192
