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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
82799-67-5
合成路线
（共 8 条）
781-17-9
4,5,9,10-四氢苯芘
+
75-36-5
乙酰氯
→
反应条件
82799-67-5
反应条件
aluminium trichloride in carbon disulfide 2 h; Ambient temperature;
参考文献
Laali, Kenneth K.; Arrica, Maria A.; Okazaki, Takao; Bunge, Scott D.
European Journal of Organic Chemistry, 2008 , # 36 p. 6093 - 6105
781-17-9
4,5,9,10-四氢苯芘
+
108-24-7
乙酸酐
→
反应条件
82799-67-5
反应条件
AlCl3, aluminium chloride in dichloromethane T=0 - 20°C; Friedel Crafts acylation; 4.5 h;
参考文献
Filichev, Vyacheslav V.; Astakhova, Irina V.; Malakhov, Andrei D.; Korshun, Vladimir A.; Pedersen, Erik B.
Chemistry - A European Journal, 2008 , vol. 14, # 32 p. 9968 - 9980
6628-98-4
4,5-二氢芘
→
反应条件
82799-67-5
反应条件
1: 95 percent / Li / tetrahydrofuran; liquid ammonia / 0.03 h / -78 °C / further reducing agent 2: 94 percent / AlCl3 / CS2 / 2 h / Ambient temperature View Scheme
参考文献
Musa, Abdallah; Sridharan, Bhama; Lee, Hyoyoung; Mattern, Daniell Lewis
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5481 - 5484
129-00-0
芘
→
反应条件
82799-67-5
反应条件
1: Li / liquid ammonia / 1 h / -78 °C 2: concd HCl / tetrahydrofuran; methanol 3: 95 percent / Li / tetrahydrofuran; liquid ammonia / 0.03 h / -78 °C / further reducing agent 4: 94 percent / AlCl3 / CS2 / 2 h / Ambient temperature View Scheme
参考文献
Musa, Abdallah; Sridharan, Bhama; Lee, Hyoyoung; Mattern, Daniell Lewis
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5481 - 5484
28862-02-4
→
反应条件
82799-67-5
反应条件
1: concd HCl / tetrahydrofuran; methanol 2: 95 percent / Li / tetrahydrofuran; liquid ammonia / 0.03 h / -78 °C / further reducing agent 3: 94 percent / AlCl3 / CS2 / 2 h / Ambient temperature View Scheme
参考文献
Musa, Abdallah; Sridharan, Bhama; Lee, Hyoyoung; Mattern, Daniell Lewis
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5481 - 5484
82799-67-5
→
反应条件
86470-96-4
反应条件
1: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 20 h / Heating 2: NaBH4 / methanol / 2 h 3: 79 percent / p-toluenesulfonic acid / benzene / 20 h / Heating 4: 63 percent / m-chloroperbenzoic acid / tetrahydrofuran / 5 h View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
82799-67-5
→
反应条件
86470-99-7
alpha-甲基-2-芘甲醇
反应条件
1: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 20 h / Heating 2: NaBH4 / methanol / 2 h View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
82799-67-5
→
反应条件
86471-00-3
反应条件
1: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 20 h / Heating 2: NaBH4 / methanol / 2 h 3: 79 percent / p-toluenesulfonic acid / benzene / 20 h / Heating View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
