1-(4-甲基苯基)-1H-吡咯合成路线 (共 31 条)
反应条件
in water T=150°C; Paal-Knorr condensation; 0.5 h; Microwave irradiation;
参考文献
Wilson, Matthew A.; Filzen, Gary; Welmaker, Gregory S.
Tetrahedron Letters, 2009 , vol. 50, # 34 p. 4807 - 4809
反应条件
copper (II) acetate monohydrate; caesium carbonate in N,N-dimethyl-formamide T=110°C; 24 h; Inert atmosphere;
参考文献
Xu, Zhong-Lin; Li, Hong-Xi; Ren, Zhi-Gang; Du, Wei-Yuan; Xu, Wei-Chang; Lang, Jian-Ping
Tetrahedron, 2011 , vol. 67, # 29 p. 5282 - 5288
反应条件
copper(l) iodide; caesium carbonate in dimethyl sulfoxide T=110°C; 24 h;
参考文献
Satish; Reddy, K. Harsha Vardhan; Ramesh; Kumar, B.S.P. Anil; Nageswar
Tetrahedron Letters, 2014 , vol. 55, # 16 p. 2596 - 2599
反应条件
copper ferrite; caesium carbonate in dimethyl sulfoxide T=110°C; 30 h; Inert atmosphere;
参考文献
Satish; Reddy, K. Harsha Vardhan; Ramesh; Kumar, B.S.P. Anil; Nageswar
Tetrahedron Letters, 2014 , vol. 55, # 16 p. 2596 - 2599
反应条件
[Cu8(H){S2P(OiPr)2}6](PF6); caesium carbonate T=105°C; Ullmann-Goldberg type coupling; 24 h;
参考文献
Wu, Cheng-Chieh; Lee, Bo-Han; Liao, Ping-Kuei; Fang, Ching-Shiang; Liu
Journal of the Chinese Chemical Society, 2012 , vol. 59, # 4 p. 480 - 484
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in dichloromethane T=100°C; 0.166667 h; microwave irradiation;
参考文献
Yang, Qian; Li, Xin-Yong; Wu, Hong; Xiao, Wen-Jing
Tetrahedron Letters, 2006 , vol. 47, # 23 p. 3893 - 3896
反应条件
MgI2 etherate in acetonitrile T=80°C; Clauson-Kaas pyrrole synthesis; chemoselective reaction;
参考文献
Tetrahedron, , vol. 67, # 5 p. 898 - 903
反应条件
MgI2 etherate in acetonitrile T=80°C; Clauson-Kaas pyrrole synthesis; chemoselective reaction;
参考文献
Tetrahedron, , vol. 67, # 5 p. 898 - 903
反应条件
palladium diacetate; potassium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in water; toluene T=80°C; Suzuki-Miyaura cross-coupling; 36 h;
参考文献
Dreher, Spencer D.; Lim, Siang-Ee; Sandrock, Deidre L.; Molander, Gary A.
Journal of Organic Chemistry, 2009 , vol. 74, # 10 p. 3626 - 3631
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79