3-苯基-1H-吡唑-5-胺合成路线 （共 39 条）
反应条件
copper(l) iodide; potassium carbonate; N,N'-dimethylcyclohexane-1,2-diamine in toluene T=110°C; 24 h;
参考文献
Antilla, Jon C.; Baskin, Jeremy M.; Barder, Timothy E.; Buchwald, Stephen L.
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5578 - 5587
反应条件
1: With sulfuric acid; sodium nitrite in water T=0°C; 0.5 h; 2: With sodium azide in water 12 h; cooling;
参考文献
Barsy, Magda A.; El-Rady, Eman A.
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 3 p. 523 - 526
反应条件
in ethanol
30 h; Heating;
参考文献
Chimichi, Stefano; Cosimelli, Barbara; Bruni, Fabrizio; Selleri, Silvia
Magnetic Resonance in Chemistry, 1992 , vol. 30, # 11 p. 1117 - 1121
参考文献
Petrov; Emelina; Firsov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 7 p. 1027 - 1032
反应条件
0.166667 h; microwave irradiation;
参考文献
Al-Shiekh, Mariam A.; El-Din, Abdellatif M. Salah; Hafez, Ebtisam A.; Elnagdi, Mohamed H.
Journal of Chemical Research, Synopses, 2004 , p. 174 - 179
反应条件
in acetic acid
20 h; Heating;
参考文献
Senga; Novinson; Wilson; Robins
Journal of Medicinal Chemistry, 1981 , vol. 24, # 5 p. 610 - 613
参考文献
Nam; Grandberg; Sorokin
Chemistry of Heterocyclic Compounds, 2002 , vol. 38, # 11 p. 1371 - 1374
反应条件
hydrogenchloride
1.5 h; Heating;
参考文献
Bellec, Christian; Lhommet, Gerard
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 6 p. 1793 - 1800
反应条件
in 1,4-dioxane
6 h; Heating;
参考文献
Pecori Vettori; Cecchi; Costanzo; Auzzi; Bruni
Farmaco, Edizione Scientifica, 1981 , vol. 36, # 6 p. 441 - 448
反应条件
1: Ambient temperature
2: melt / 180 °C
3: NaOH / H2O; various solvent(s) / Heating
View Scheme
参考文献
Pecori Vettori; Cecchi; Costanzo; Auzzi; Bruni
Farmaco, Edizione Scientifica, 1981 , vol. 36, # 6 p. 441 - 448
