3-苯基-1H-吡唑-5-胺合成路线 （共 39 条）
反应条件
hydrazine hydrate in methanol T=120°C; 0.666667 h; microwave irradiation;
参考文献
Bagley, Mark C.; Davis, Terence; Dix, Matthew C.; Widdowson, Caroline S.; Kipling, David
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 22 p. 4158 - 4164
反应条件
hydrazine hydrate T=80°C; 0.333333 h;
参考文献
Fomum, Z. Tanee; Landor, Stephen R.; Landor, Phyllis D.; Mpango, George W. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2997 - 3001
反应条件
hydrazine hydrate in isopropyl alcohol 0.5 h; Heating;
参考文献
Rusinov, V. L.; Myasnikov, A. V.; Chupakhin, O. N.; Aleksandrov, G. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 5 p. 530 - 533
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 5 p. 665 - 668
反应条件
hydrazine hydrate in ethanol 5 h; Heating;
参考文献
Hartmann, Horst; Liebscher, Juergen
Synthesis, 1984 , # 3 p. 276 - 277
反应条件
montmorillonite K-10; hydrazine hydrate in dichloromethane 22 h; ultrasound bath;
参考文献
Braibante, Mara E. F.; Braibante, Hugo T. S.; Da Roza, Juliano K.; Henriques, Danielle M.; De Carvalho Tavares, Luciana
Synthesis, 2003 , # 8 p. 1160 - 1162
反应条件
in ethanol T=100°C; 15 h;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 38, # 5 p. 581 - 585
反应条件
1.1: lithium diisopropylamide / tetrahydrofuran / -78 °C 1.2: tetrahydrofuran / -78 - 20 °C 2.1: hydrazine monohydrate / ethanol / 5 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 14, # 22 p. 7501 - 7511
反应条件
1: 78 percent / montmorillonite K-10; NH3 / CH2Cl2 / 22 h / ultrasound bath 2: 45 percent / NH2NH2*H2O; montmorillonite K-10 / CH2Cl2 / 22 h / ultrasound bath View Scheme
参考文献
Synthesis, , # 8 p. 1160 - 1162
反应条件
1: NaNH2 / toluene / 10 h / 0 - 20 °C 2: 78 percent / montmorillonite K-10; NH3 / CH2Cl2 / 22 h / ultrasound bath 3: 45 percent / NH2NH2*H2O; montmorillonite K-10 / CH2Cl2 / 22 h / ultrasound bath View Scheme
参考文献
Synthesis, , # 8 p. 1160 - 1162
反应条件
1.1: dihydrogen peroxide; acetic acid / dichloromethane / 5 h / 45 °C 2.1: hydrazine hydrate / ethanol / 2.33 h / -5 °C / Reflux 2.2: 1 h / 55 °C View Scheme
参考文献
Heterocyclic Communications, , vol. 17, # 3-4 p. 139 - 145
