反-1,2-环丙烷二羧酸二甲酯合成路线 （共 25 条）
反应条件
sodium hydride in dimethyl sulfoxide 12 h;
参考文献
Baldwin, John E.; Cianciosi, Steven J.
Journal of the American Chemical Society, 1992 , vol. 114, # 24 p. 9401 - 9408
反应条件
sodium methylate 1.) RT, 16 h, 2.) methanol, 75-80 deg C, 14 h;
参考文献
Skatteboel, Lars; Stenstroem, Yngve
Acta Chemica Scandinavica, 1989 , vol. 43, # 1 p. 93 - 96
反应条件
tetrabutylammomium bromide; tetra-(n-butyl)ammonium iodide; triphenylphosphine in acetonitrile T=20°C; Electrochemical reaction;
参考文献
Sengmany, Stephane; Leonel, Eric; Paugam, Jean Paul; Nedelec, Jean-Yves
Tetrahedron, 2002 , vol. 58, # 2 p. 271 - 277
反应条件
sulfuric acid 24 h; Reflux;
参考文献
Hugentobler, Katharina G.; Rebolledo, Francisca
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 4 p. 615 - 623
反应条件
titanium tetrachloride in dichloromethane 1) 0 deg C, 2) 20 deg C, l h;
参考文献
Wallace, I. H. M.; Chan, T. H.
Tetrahedron, 1983 , vol. 39, # 6 p. 847 - 854
反应条件
(PPh3)2N(1+)*Cr(CO)4NO(1-) in dichloromethane T=-78°C; Yield given;
参考文献
Canadian Journal of Chemistry, , vol. 71, # 2 p. 258 - 262
反应条件
in various solvent(s) Ambient temperatureelectrolysis (Bu4NBF4/Bu4NI, Al anode, steel cathode);
参考文献
Lu, Yu-Wei; Nedelec, Jean-Yves; Folest, Jean-Claude; Perichon, Jacques
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2503 - 2507
反应条件
sodium hydride in tetrahydrofuran
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 20, p. 2593 - 2602
反应条件
1: diethyl ether 2: (PPh3)2N(1+)*Cr(CO)4NO(1-) / CH2Cl2 / -78 °C View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 71, # 2 p. 258 - 262
反应条件
(i) NaH, DMSO, (ii) /BRN= 774590/; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 90, p. 6852 - 6854
