顺-1,2-环丙烷二羧酸二甲酯合成路线 （共 23 条）
反应条件
sodium methylate 1.) RT, 16 h, 2.) methanol, 75-80 deg C, 14 h;
参考文献
Skatteboel, Lars; Stenstroem, Yngve
Acta Chemica Scandinavica, 1989 , vol. 43, # 1 p. 93 - 96
反应条件
hydrogenchloride; sodium hydroxide; dihydrogen peroxide in methanol 1.) -70 deg C, 2) -30 deg C, 3.) 0 deg C, several hours;
参考文献
Takaya, H.; Suzuki, T.; Kumagai, Y.; Hosoya, M.; Kawauchi, H.; Noyori, R.
Journal of Organic Chemistry, 1981 , vol. 46, # 14 p. 2854 - 2861
反应条件
in diethyl ether T=0°C;
参考文献
Journal of the American Chemical Society, , vol. 126, # 39 p. 12353 - 12362
反应条件
copper(II) sulfate T=70°C; 4.5 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 46, # 14 p. 2854 - 2861
反应条件
(PPh3)2N(1+)*Cr(CO)4NO(1-) in acetonitrile T=-40°C; other solvents and temperatures; same reaction with meso isomer; Mechanism;
参考文献
Canadian Journal of Chemistry, , vol. 71, # 2 p. 258 - 262
反应条件
tetraethylammonium chloride; tetraethylammonium tetrafluoroborate; triphenylphosphine; nickel dichloride in acetonitrile electrolysis; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Russian Journal of General Chemistry, , vol. 67, # 2 p. 257 - 259
反应条件
sulfuric acid Fischer esterification; 2 h; Heating;
参考文献
Tetrahedron Asymmetry, , vol. 11, # 17 p. 3569 - 3584
反应条件
1: methanol / Heating 2: diethyl ether View Scheme
参考文献
Helvetica Chimica Acta, , vol. 66, # 8 p. 2501 - 2511
参考文献
Helvetica Chimica Acta, , vol. 66, # 8 p. 2501 - 2511
反应条件
sodium iodide; niobium bromide; zinc 1.) acetonitrile, RT, 2.) acetonitrile, RT, 24 h; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 56, # 6 p. 1592 - 1597
