(S)-3-羟基丁酸(+)-叔丁酯合成路线 (共 8 条)
反应条件
hydrogen; C50H44Cl2N2O8P4Ru(4-)*Zr(4+) in methanol T=20°C; P=72402.6 Torr; 20 h; Product distribution / selectivity;
参考文献
Lin, Wenbin; Hu, Aiguo; Ngo, Helen L.
Patent: US2004/192543 A1, 2004 ;
Location in patent: Page/Page column 9 ;
反应条件
Pseudomonas cepacia lipase immobilized on ceramic; potassium tert-butylate; sodium carbonate; [2,3,4,5-Ph4(η5-C4CNH(i-Pr))]Ru(CO)2Cl in toluene T=25°C; 120 h;
参考文献
Choi, Jun Ho; Choi, Yoon Kyung; Kim, Yu Hwan; Park, Eun Sil; Kim, Eun Jung; Kim, Mahn-Joo; Park, Jaiwook
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 1972 - 1977
反应条件
polymer-supported Geotrichum candidum dried cells; β-NADP+; (EMIM) tetrafluoroborate T=30°C; 16 h;
参考文献
Matsuda, Tomoko; Marukado, Ryo; Mukouyama, Masaharu; Harada, Tadao; Nakamura, Kaoru
Tetrahedron Asymmetry, 2008 , vol. 19, # 19 p. 2272 - 2275
参考文献
Solladie, Guy; Almario, Antonio
Tetrahedron Letters, 1992 , vol. 33, # 18 p. 2477 - 2480
反应条件
1: 68 percent / ZnCl2, HAl(iBu)2 / tetrahydrofuran / -78 °C 2: 85 percent / Raney Nickel View Scheme
参考文献
Tetrahedron Letters, , vol. 33, # 18 p. 2477 - 2480
反应条件
1: m-chloroperbenzoic acid / CH2Cl2 / -78 °C 2: aluminium amalgam View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 44 p. 5083 - 5086
反应条件
sodium carbonate in methanol Ambient temperature; Yield given;
参考文献
Helvetica Chimica Acta, , vol. 81, # 12 p. 2430 - 2461
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; 10 h;
参考文献
Yang, Dan; Zhang, Yu-Hui; Li, Bing; Zhang, Dan-Wei
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7577 - 7581