反应条件
1.1: benzotriazol-1-ol; N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide / N,N-dimethyl-formamide / 0 - 20 °C
1.2: 0 - 20 °C
2.1: diisobutylaluminium hydride / tetrahydrofuran / 3.17 h / -78 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Inoue, Takayuki; Morita, Masataka; Tojo, Takashi; Nagashima, Akira; Moritomo, Ayako; Imai, Keisuke; Miyake, Hiroshi
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 9 p. 2478 - 2494
