N,N,4-三甲基苯胺 N-氧化物合成路线 (共 11 条)
反应条件
1H-imidazole; 5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride in chloroform T=25°C; 0.183333 h;
参考文献
Fujimori, Ken; Takata, Toshikazu; Fujiwara, Seiichi; Kikuchi, Osamu; Oae, Shigeru
Tetrahedron Letters, 1986 , vol. 27, # 14 p. 1617 - 1620
反应条件
1: With N,N-dimethylthiocarbamoyl chloride in dichloromethane T=20°C; 2 h; 2: in acetonitrile 3 h; Reflux;
参考文献
Caliskan, Hafize; Zaim, Oemer
Synthetic Communications, 2010 , vol. 40, # 20 p. 3078 - 3083
反应条件
in acetonitrile 3 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 3 p. 527 - 530
反应条件
T=140°C; pyrolysed under various conditions; Mechanism;
参考文献
Demir, Tuersen; Shaw, Robert A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1547 - 1552
反应条件
1H-imidazole; 5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride in chloroform T=25°C; 0.183333 h;
参考文献
Fujimori, Ken; Takata, Toshikazu; Fujiwara, Seiichi; Kikuchi, Osamu; Oae, Shigeru
Tetrahedron Letters, 1986 , vol. 27, # 14 p. 1617 - 1620
反应条件
epoxysulfonyl fluoride in trifluoroacetic acid T=-10°C; Yields of byproduct given;
参考文献
Smith, John R. Lindsay; Linford, Janet M.; McKeer, Linda C.; Morris, Paul M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1099 - 1106
反应条件
water; epoxysulfonyl fluoride 1.) TFA, -10 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Smith, John R. Lindsay; Linford, Janet M.; McKeer, Linda C.; Morris, Paul M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1099 - 1106
反应条件
sodium hydroxide; epoxysulfonyl fluoride 1.) TFA, -10 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Smith, John R. Lindsay; Linford, Janet M.; McKeer, Linda C.; Morris, Paul M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1099 - 1106
反应条件
epoxysulfonyl fluoride in trifluoroacetic acid T=-10°C; Yields of byproduct given;
参考文献
Smith, John R. Lindsay; Linford, Janet M.; McKeer, Linda C.; Morris, Paul M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1099 - 1106
反应条件
sodium hydroxide; epoxysulfonyl fluoride 1.) TFA, -10 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Smith, John R. Lindsay; Linford, Janet M.; McKeer, Linda C.; Morris, Paul M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1099 - 1106