1.1: formic acid; dihydrogen peroxide / water / 4 h / 20 °C 2.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 0.5 h / -78 °C 2.2: 3 h / -78 - 20 °C View Scheme
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1.1: formic acid; dihydrogen peroxide / water / 4 h / 20 °C 2.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 0.5 h / -78 °C 2.2: 3 h / -78 - 20 °C 3.1: potassium hydroxide / water / 20 °C 4.1: hydrogenchloride; water / 1 h / Reflux 5.1: ammonia / water / 5 h / Heating; High-pressure flask 6.1: trichlorophosphate / 1 h / 110 °C / Microwave irradiation View Scheme
