hydrogenchloride in tetrahydrofuran dry oxygen-free solvents, evacuated glass ampoules;

in diethyl ether dry oxygen-free solvents, evacuated glass ampoules; addn. of Ge-compd. in Et2O to Hg-compd. in Et2O, react. at 20°C (few min); sepn. of metallic Hg from soln., removal of Et2O in vac., sublimation (20°C, 0.01 mm); elem. anal.;