2-羟基-3-甲基苯甲醛合成路线 （共 54 条）
反应条件
1.1: magnesium / diethyl ether / 1.5 h / Reflux
1.2: 2 h / 0 °C / Reflux
2.1: air; Mn3O4 nanoparticles / N,N-dimethyl-formamide / 6 h / 80 °C
View Scheme
参考文献
Sun, Huayin; Zhang, Yonghui; Guo, Fengfeng; Yan, Yizhe; Wan, Changfeng; Zha, Zhenggen; Wang, Zhiyong
European Journal of Organic Chemistry, 2012 , # 3 p. 480 - 483
反应条件
potassium carbonate in DMF (N,N-dimethyl-formamide)
T=20 - 45°C; 30 h;
参考文献
AVENTIS PHARMACEUTICALS INC.
Patent: WO2005/111025 A1, 2005 ;
Location in patent: Page/Page column 90 ;
WO 2005/111025 A1
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 26 h;
参考文献
CHUGAI SEIYAKU KABUSHIKI KAISHA
Patent: EP1783110 A1, 2007 ;
Location in patent: Page/Page column 42 ;
反应条件
potassium carbonate in dimethyl sulfoxide
参考文献
Nippon-Soda
Patent: DE2252818 , 1974 ;
Chem.Abstr., 1974 , vol. 81, # 25407
