反应条件
1: 1.) Raney nickel, 2.) H2 / 2.) 10percent Pd/C / 1.) EtOH, reflux, 48 h, 2.) 40 psi, 2 h 2: 76 percent / KOH / ethane-1,2-diol; H2O / 12 h / Heating 3: oxalyl chloride / 6 h / Ambient temperature View Scheme
参考文献
Wenkert, Ernest; Davis, Linda L.; Mylari, Banavara L.; Solomon, Mary F.; Silva, Roberto R. da; et al.
Journal of Organic Chemistry, 1982 , vol. 47, # 17 p. 3242 - 3247
