2-(羟基亚甲基)环己酮合成路线 （共 42 条）
反应条件
4-toluenesulfonyl azide; potassium carbonate 0.0833333 h;
参考文献
Rao, Y. Koteswar; Nagarajan, M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 735 - 737
反应条件
1: sodium acetate / methanol; water View Scheme
参考文献
Chakraborty, Suchandra; Chattopadhyay, Gautam; Saha, Chandan
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 2 p. 331 - 338
参考文献
Dreiding; Nickel
Journal of the American Chemical Society, 1954 , vol. 76, p. 3965,3967
反应条件
(i) NH2OH*HCl, aq. HCl, EtOH, (ii) NaOMe, MeOH, (iii) NH2OH*HCl, aq. NaOH; Multistep reaction;
参考文献
Kloetzer,W. et al.
Monatshefte fuer Chemie, 1970 , vol. 101, p. 1109 - 1122
反应条件
potassium hydroxide in methanol 5 h; Ambient temperature;
参考文献
Ravikumar, V. T.; Sathyamoorthi, G.; Thangaraj, K.; Rajagopalan, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 959
反应条件
potassium hydroxide in methanol 1) 5 h, r.t., then 2 h, reflux;
参考文献
Ravikumar, V. T.; Sathyamoorthi, G.; Thangaraj, K.; Rajagopalan, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 959
反应条件
methanol; hydrazine hydrate
参考文献
Ainsworth
Organic Syntheses, 1963 , vol. Coll. Vol. IV, p. 536,538
反应条件
2: aqueous KOH 3: soda lime / Erhitzen unter vermindertem Druck View Scheme
参考文献
Basu
Justus Liebigs Annalen der Chemie, 1934 , vol. 512, p. 131,132
Justus Liebigs Annalen der Chemie, 1937 , vol. 530, p. 131,132
反应条件
pyridine in tetrahydrofuran
6 h; Ambient temperature;
参考文献
Pinhey, John T.; Rowe, Bruce A.
Australian Journal of Chemistry, 1983 , vol. 36, # 4 p. 789 - 794
反应条件
potassium hydroxide in methanol
1) 5 h, r.t., then 2 h, reflux;
参考文献
Ravikumar, V. T.; Sathyamoorthi, G.; Thangaraj, K.; Rajagopalan, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 959
