(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium; 5,17-bis[(3-(2,6-diisopropylphenyl)imidazolium)methyl]-25,26,27,28-tetrapropoxycalix[4]arene dichloride in water T=45°C; 24 h; optical yield given as percent de;
参考文献
Brendgen, Thomas; Fahlbusch, Tilmann; Frank, Markus; Schuehle, Daniel T.; Sessler, Miriam; Schatz, Juergen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 3 p. 303 - 307
hydrogenchloride; diethyl ether; water in ethanol 16 h; Inert atmosphereReflux;
参考文献
Stehouwer, Jeffrey S.; Daniel, Lauryn M.; Chen, Ping; Voll, Ronald J.; Williams, Larry; Plott, Susan J.; Votaw, John R.; Owens, Michael J.; Howell, Leonard; Goodman, Mark M.
Journal of Medicinal Chemistry, 2010 , vol. 53, # 15 p. 5549 - 5557
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in water; tert-butyl alcohol T=32°C; 2.5 h; optical yield given as percent de;
参考文献
Journal of the American Chemical Society, , vol. 132, # 47 p. 16805 - 16811
