2-甲基-2-丙烯基乙酸酯合成路线 (共 57 条)
反应条件
ruthenium trichloride T=40°C; 0.5 h; Inert atmosphereIonic liquid;
参考文献
Xi, Zhiwen; Hao, Wenyan; Wang, Pingping; Cai, Mingzhong
Molecules, 2009 , vol. 14, # 9 p. 3528 - 3537
反应条件
Wilkinson's catalyst in toluene T=130°C; 55 h;
参考文献
Journal of the American Chemical Society, , vol. 125, # 4 p. 886 - 887
反应条件
in 1-methyl-pyrrolidin-2-one T=120°C; 0.5 h; Heating / reflux;
参考文献
US6348597 B2, ;
Page column 87 ;
反应条件
in acetic acid T=100°C; 48 h;
参考文献
Kartashov, V. R.; Skorobogatova, E. V.; Akimkina, N. F.; Zefirov, N. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 32 - 35
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 1 p. 38 - 42
反应条件
pyridine T=5°C; 0.25 h;
参考文献
Moorlag, Henk; Vries, Johannes G. de; Kaptein, Bernard; Schoemaker, Hans E.; Kamphuis, Johan; Kellogg, Richard M.
Recueil des Travaux Chimiques des Pays-Bas, 1992 , vol. 111, # 3 p. 129 - 137
反应条件
1: 2-methyl-2-propenal; diethylzinc With (1R,2S)-(+)-1-cyclohexyl-2-phenyl-2-(N-morpholino)ethanol in hexane; toluene T=20°C; 3 h; 2: acetic anhydride in hexane; toluene Further stages. Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 4, # 13 p. 2133 - 2136
参考文献
Journal of the American Chemical Society, , vol. 93, # 20 p. 5107 - 5111
反应条件
lipase PS-D T=25°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 44, # 16 p. 3267 - 3269
反应条件
hydrogenchloride T=0°C;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 32 - 35
Zhurnal Organicheskoi Khimii, , vol. 18, # 1 p. 38 - 42
参考文献
Tetrahedron, , vol. 26, p. 477 - 495