(2-羟基苯甲酰亚甲基)三苯基膦合成路线 （共 8 条）
反应条件
pyridine in toluene 5 h; Heating;
参考文献
Hercouet, A.; Le Corre, M.; Le Floc'h, Y.
Synthesis, 1982 , # 7 p. 597 - 598
反应条件
pyridine in toluene 5 h; Heating;
参考文献
Hercouet, A.; Le Corre, M.; Le Floc'h, Y.
Synthesis, 1982 , # 7 p. 597 - 598
反应条件
1: 81 percent / bromine / CCl4 / Heating
2: 2.) aq, HBr / 1.) Toluene, reflux, 1 h, 2.) reflux, 1 h
View Scheme
参考文献
Hercouet, A.; Le Corre, M.; Le Floc'h, Y.
Synthesis, 1982 , # 7 p. 597 - 598
反应条件
1: 96 percent / benzene
2: 65 percent / NaOEt / ethanol
View Scheme
参考文献
Shvets, A. A.; Khoruzhaya, I. A.; Kokorev, G. I.; Safaryan, G. P.; Kogan, V. A.
Russian Journal of General Chemistry, 1995 , vol. 65, # 1.1 p. 43 - 45
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 1 p. 53 - 55
反应条件
1: 96 percent / benzene
2: 65 percent / NaOEt / ethanol
View Scheme
参考文献
Shvets, A. A.; Khoruzhaya, I. A.; Kokorev, G. I.; Safaryan, G. P.; Kogan, V. A.
Russian Journal of General Chemistry, 1995 , vol. 65, # 1.1 p. 43 - 45
Zhurnal Obshchei Khimii, 1995 , vol. 65, # 1 p. 53 - 55
反应条件
hydrogen bromide
1.) Toluene, reflux, 1 h, 2.) reflux, 1 h; Yield given. Multistep reaction;
参考文献
Hercouet, A.; Le Corre, M.; Le Floc'h, Y.
Synthesis, 1982 , # 7 p. 597 - 598
反应条件
n-butyllithium
1.) hexane, THF, r.t., 3 h, 2.) THF, 60 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Zammattio; Brion; Le Baut; Ducrey
Synthesis, 1992 , # 4 p. 375 - 376
反应条件
pyridine in toluene
5 h; Heating;
参考文献
Hercouet, A.; Le Corre, M.; Le Floc'h, Y.
Synthesis, 1982 , # 7 p. 597 - 598
