3-氟-4-氨基苯硼酸频哪醇酯合成路线 （共 7 条）
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium acetate in dimethyl sulfoxide T=85°C; 4.5 h; Inert atmosphere;
参考文献
US2013/178472 A1, ;
Paragraph 0239; 0240 ;
反应条件
potassium acetate; 1,1'-bis-(diphenylphosphino)ferrocene in 1,4-dioxane T=80°C;
参考文献
WO2007/64883 A2, ;
Page/Page column 199-200 ;
反应条件
5 palladium on charcoal; hydrogen in methanol T=20°C; P=760.051 Torr; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 79, # 5 p. 1979 - 1988
反应条件
1: With hydrogenchloride in 1,4-dioxane; dichloromethane T=30°C; 2.5 h; 2: With sodium hydrogencarbonate in water Product distribution / selectivity;
参考文献
WO2007/147574 A1, ;
Page/Page column 56 ;
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) chloroform complex; triethylamine in 1,4-dioxane Heating;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 5 p. 1221 - 1227
反应条件
1: 2-(4-biphenylyl)-5-phenyl-oxazole; tert.-butylnitrite / acetonitrile / 4 h / 20 °C 2: 5 palladium on charcoal; hydrogen / methanol / 4 h / 20 °C / 760.05 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 79, # 5 p. 1979 - 1988
反应条件
1: 2-(4-biphenylyl)-5-phenyl-oxazole; tert.-butylnitrite / acetonitrile / 4 h / 20 °C 2: 5 palladium on charcoal; hydrogen / methanol / 4 h / 20 °C / 760.05 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 79, # 5 p. 1979 - 1988
