1: With magnesium; ethylene dibromide in tetrahydrofuran
T=20°C; Inert atmosphere;
2: With phosphorus trichoride in tetrahydrofuran
Inert atmosphereCooling;
参考文献
Nawara-Hultzsch, Agnieszka J.; Skopek, Katrin; Shima, Takanori; Barbasiewicz, Micha; Hess, Gisela D.; Skaper, Dirk; Gladysz, John A.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2010 , vol. 65, # 3 p. 414 - 424