1: With sulfuric acid in water
T=20°C; 0.166667 h; Inert atmosphere;
2: With (NH4)2S2O8; silver nitrate
T=90°C; 2 h; Inert atmosphere;
参考文献
F. HOFFMANN-LA ROCHE AG; HOFFMANN-LA ROCHE INC.; HUBY, Nicholas John Silvester; LOPEZ-TAPIA, Francisco Javier; SO, Sung-Sau
Patent: WO2014/90715 A1, 2014 ;
Location in patent: Page/Page column 45 ;
1: With sodium tetrahydroborate; sodium hydroxide in water
T=0 - 20°C; 16.5 h; Inert atmosphereSchlenk technique;
2: With hydrogenchloride in water
Inert atmosphereSchlenk technique;
参考文献
Nitsch, Dominik; Huber, Stefan M.; Poethig, Alexander; Narayanan, Arjun; Olah, George A.; Prakash, G. K. Surya; Bach, Thorsten
Journal of the American Chemical Society, 2014 , vol. 136, # 7 p. 2851 - 2857