1,1,2,2-四甲基乙硅烷合成路线 (共 19 条)
反应条件
Mg-anode; stainless steel cathode in tetrahydrofuran 192 h; Electrolysis;
参考文献
Grogger, Christa; Loidl, Bernhard; Stueger, Harald; Kammel, Thomas; Pachaly, Bernd
Journal of Organometallic Chemistry, 2006 , vol. 691, # 1-2 p. 105 - 110
反应条件
tri-n-butyl-tin hydride; benzildianil
参考文献
Journal of Organometallic Chemistry, , vol. 533, # 1-2 p. 73 - 77
反应条件
lithium perchlorate in tetrahydrofuran Electrolysis;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 1-2 p. 105 - 110
反应条件
in toluene byproducts: H2; argon atmosphere or vac.; heating mixt. of V-complex and org. compd. (molar ratio 1:1) and toluene (evac. ampul, 70-100°C, 30-40 h), evolved hydrogen drawing off, soln. decanting; ppt. suction-filtration off, drying, filtrate transcondensation and chromy. (GLC) leads to org. byproducts; elem. anal.;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 52, p. 1175 - 1178
Zhurnal Obshchei Khimii, , vol. 52, p. 1334 - 1338
反应条件
lithium aluminium tetrahydride
参考文献
Monatshefte fuer Chemie, , vol. 105, p. 671 - 683
反应条件
Ph3P(1+)MeI; tri-n-butyl-tin hydride
参考文献
Journal of Organometallic Chemistry, , vol. 527, # 1-2 p. 117 - 124
参考文献
Angewandte Chemie, , vol. 75, p. 516 - 524
反应条件
tetra-n-butylammonium tetrafluoroborate in tetrahydrofuran Electrolysis; Product distribution; Further Variations:Reagents;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 1-2 p. 105 - 110
反应条件
T=141.4°C; P=46 Torr; 0.5 h; Irradiationvar. temp.; other silicon compounds; Product distributionMechanism;
参考文献
Journal of Organometallic Chemistry, , vol. 206, # 2 p. 149 - 158
反应条件
2-Butyne Ambient temperatureIrradiationconcentration dependence; Product distribution;
参考文献
Journal of the Chemical Society - Faraday Transactions, , vol. 93, # 6 p. 1071 - 1078