2-甲基-1-丁烯-3-酮合成路线 （共 116 条）
参考文献
Colonge; Pichat
Bulletin de la Societe Chimique de France, 1949 , p. 177,183
反应条件
1: Raney nickel; ethanol / 20 - 32 °C / Hydrogenation.unter Druck View Scheme
参考文献
Hurd; McPhee
Journal of the American Chemical Society, 1949 , vol. 71, p. 400
反应条件
n-butyllithium; lithium diisopropyl amide 1.) hexane, diethylether, -60 deg C, 15 min, 2.) 5 min; Yield given. Multistep reaction;
参考文献
Baeckstroem, Peter; Li, Lanna
Synthetic Communications, 1990 , vol. 20, # 10 p. 1481 - 1485
反应条件
1: (i) MeOH, (ii) aq. K2CO3 2: HCl / diethyl ether 3: aq. H2SO4 4: aq. Ba(OH)2 View Scheme
参考文献
Edwards,J.D. et al.
Journal of Heterocyclic Chemistry, 1967 , vol. 4, p. 487 - 490
反应条件
sulfuric acid T=60 - 80°C;
参考文献
Hagemeyer
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 769
反应条件
sulfuric acid bei Siedetemperatur;
参考文献
Hagemeyer; Hull
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 2921
Full Text Show Details
Carbide and Carbon Chem.Corp.
Patent: US2467095 , 1947 ;
Full Text Show Details
Carbide and Carbon Chem.Corp.
Patent: US2466737 , 1944 ;
反应条件
ozone in polyethylene T=-75°C; 3.5 h;
参考文献
Griesbaum, Karl; Greunig, Hans-Joachim; Volpp, Willi; Jung, In-Chan
Chemische Berichte, 1991 , vol. 124, # 4 p. 947 - 956
反应条件
ozone in dichloromethane-d2 T=-78°C; Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 124, # 4 p. 947 - 956
反应条件
ozone in polyethylene T=-75°C; 4 h; Further byproducts given;
参考文献
Chemische Berichte, , vol. 124, # 4 p. 947 - 956
反应条件
diethyl ether
und Zersetzen des Reaktionsprodukts mit starker KOH unter Luehlung durch Kaeltemischung;
参考文献
Ogloblin
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 2157
Chem.Abstr., 1949 , p. 3777
