in xylene starting material in soln. heated at 150°C for 6h;
参考文献
Vyshinskaya, L. I.; Timoshenko, S. Ya.; Vishnyakova, T. A.
Journal of General Chemistry USSR (English Translation), 1990 , vol. 60, p. 1729 - 1733
Zhurnal Obshchei Khimii, 1990 , vol. 60, p. 1937 - 1942
tetrakis(triphenylphosphine) palladium(0) in toluene byproducts: ((CH3)3Si)2; mixt. of 2 equiv of isonitrile and 5 equiv of organosilylstannane and 0.06 equiv of Pd-complex was heated in toluene at 60°C for 3 h under Ar; distd.; elem. anal.;;
参考文献
Ito, Yoshihiko; Bando, Takashi; Matsuura, Takaharu; Ishikawa, Mitsuo
Journal of the Chemical Society, Chemical Communications, 1986 , # 12 p. 980 - 981
in neat (no solvent) 2 equiv of Sn deriv. and 1 equiv of the cycloalkene heating at 180°C for 64 h under Ar; isolated by gas chromy. at 230°C; identified by NMR and mass spectra;
参考文献
Quintard, Jean-Paul; Degueil-Castaing, Marie; Barbe, Bernard; Petraud, Michel
Journal of Organometallic Chemistry, 1982 , vol. 234, # 1 p. 41 - 62
in tetrahydrofuran Electrolysis; electrolyte 0.4 M LiClO4 in THF; electrolysis carried out galvanostatically at 25-28°C in atm. of dry N2; hexane added to electrolyte, ppt. filtered off, filtrate analyzed for the products by GC;
