1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Inert atmosphere; 2: With boric acid trimethyl ester in tetrahydrofuran; hexane T=-78 - 20°C; Inert atmosphere; 3: With hydrogenchloride; water in tetrahydrofuran; hexane T=20°C; 0.5 h; Inert atmosphere;
参考文献
Kong, Yali; Wang, Kan; Edler, Michael C.; Hamel, Ernest; Mooberry, Susan L.; Paige, Mikell A.; Brown, Milton L.
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 2 p. 971 - 977
