1,1,1,2-四氯丙烷合成路线 （共 15 条）
反应条件
sulfuryl dichloride; 2,2'-azo-bisisobutyronitrile
T=55 - 60°C;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; KRUPER, William J.; FISH, Barry; LAITAR, David Stephen
Patent: WO2012/166394 A1, 2012 ;
Location in patent: Page/Page column 18-19 ;
反应条件
hydrogenchloride; iron(III) chloride
T=50°C;
参考文献
Kharasch; Rossin; Fields
Journal of the American Chemical Society, 1941 , vol. 63, p. 2560
Full Text Show Details
de la Mare; Vernon
Journal of the Chemical Society, 1952 , p. 3629
反应条件
beim Chlorieren zunaechst im Sonnenlicht in der Dampfphase, dann in fluessiger Phase unter Kuehlung;
参考文献
Henne; Whaley
Journal of the American Chemical Society, 1942 , vol. 64, p. 1157
反应条件
chlorine; iron(III) chloride
参考文献
du Pont de Nemours and Co.
Patent: US2097442 , 1935 ;
反应条件
diacetyl peroxide
6 h; Heating;
参考文献
Ol'dekop, Yu. A.; Kaberdin, R. V.; Buslovskaya, E. E.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 222 - 225
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 2 p. 272 - 275
参考文献
Kharasch; Rossin; Fields
Journal of the American Chemical Society, 1941 , vol. 63, p. 2560
反应条件
diacetyl peroxide
6 h; Heating; Further byproducts given;
参考文献
Ol'dekop, Yu. A.; Kaberdin, R. V.; Buslovskaya, E. E.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 222 - 225
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 2 p. 272 - 275
反应条件
Chlorieren, zunaechst im Sonnenlicht in der Dampfphase, dann in fluessiger Phase unter Kuehlung; Produkt 5: 1.1.1.3-Tetrachlor-propan;
参考文献
Henne; Whaley
Journal of the American Chemical Society, 1942 , vol. 64, p. 1157
参考文献
Krenzel' et al.
Doklady Akademii Nauk SSSR, 1956 , vol. 107, p. 89
Chem.Abstr., 1956 , p. 13713
Full Text Show Details
Toptschiew et al.
Doklady Akademii Nauk SSSR, 1957 , vol. 116, p. 800,801
Doklady Chemistry, 112-117<1957>921,923
参考文献
Henry
Recueil des Travaux Chimiques des Pays-Bas, 1905 , vol. 24, p. 332,337
Chem. Zentralbl., 1905 , vol. 76, # I p. 1697
