lithium aluminium tetrahydride in diethyl ether
T=0°C; Reduction; 0.5 h;
参考文献
Jones, Graham B.; Wright, Justin M.; Plourde, Gary W.; Hynd, George; Huber, Robert S.; Mathews, Jude E.
Journal of the American Chemical Society, 2000 , vol. 122, # 9 p. 1937 - 1944
1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -10 °C
1.2: tetrahydrofuran / 0 - 25 °C
2.1: LiAlH4 / diethyl ether / 0.5 h / 0 °C
View Scheme
参考文献
Jones, Graham B.; Wright, Justin M.; Plourde, Gary W.; Hynd, George; Huber, Robert S.; Mathews, Jude E.
Journal of the American Chemical Society, 2000 , vol. 122, # 9 p. 1937 - 1944