4-溴-1,8-萘二甲酸酐合成路线 （共 43 条）
反应条件
1: With bromine; potassium hydroxide in water T=0 - 60°C; 18 h; 2: With sulfuric acid in water T=20°C; Reflux;
参考文献
Rotstein, Benjamin H.; Mourtada, Rida; Kelley, Shana O.; Yudin, Andrei K.
Chemistry - A European Journal, 2011 , vol. 17, # 44 p. 12257 - 12261
反应条件
sodium dichromate in water; acetic acid Oxidation; 12 h; Heating;
参考文献
Alaei, Parvaneh; Rouhani, Shohre; Gharanjig, Kamaladin; Ghasemi, Jahanbakhsh
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 90, p. 85 - 92
反应条件
chromium(VI) oxide in acetic acid T=80°C; 1 h;
参考文献
Solodar', S. L.; Vinogradov, L. M.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1102 - 1104
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1275 - 1277
反应条件
1: chloroform; bromine 2: glacial acetic acid; sodium dichromate / 50 - 70 °C / Behandeln des Reaktionsprodukts in Wasser View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 327, p. 86
反应条件
phosphorus pentabromide T=190 - 200°C;
参考文献
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, , vol. <A>, p. 420
Chem. Zentralbl., , vol. 100, # I p. 650
反应条件
1: 0.29 g / ammonium acetate / 2 h / 130 - 140 °C 2: 1)nitrosylsulfuric acid, sodium nitrite, 2) cuprous bromide, 48percent hydrobromic acid / 1) acetic acid, 1 - 5 deg C, 20 min, 2) 1 - 5 deg C, 20 min 3: 13 percent / CrO3 / acetic acid / 1 h / 80 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 1102 - 1104
Zhurnal Organicheskoi Khimii, , vol. 16, # 6 p. 1275 - 1277
反应条件
1: 1)nitrosylsulfuric acid, sodium nitrite, 2) cuprous bromide, 48percent hydrobromic acid / 1) acetic acid, 1 - 5 deg C, 20 min, 2) 1 - 5 deg C, 20 min 2: 13 percent / CrO3 / acetic acid / 1 h / 80 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 1102 - 1104
Zhurnal Organicheskoi Khimii, , vol. 16, # 6 p. 1275 - 1277
参考文献
Zhurnal Organicheskoi Khimii, , vol. 2, # 12 p. 2206 - 2208,2162 - 2164
反应条件
1: Na2Cr2O7, AcOH / Heating 2: Ac2O View Scheme
参考文献
Zhurnal Organicheskoi Khimii, , vol. 2, # 12 p. 2206 - 2208,2162 - 2164
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 229, p. 624
