1,8-二羟基-4,5-二硝基蒽醌合成路线 (共 6 条)
反应条件
sulfuric acid; nitric acid; boric acid T=25°C;
参考文献
Chang; Cheng
Synthetic Communications, 1995 , vol. 25, # 13 p. 1893 - 1900
反应条件
sulfuric acid; nitric acid; boric acid T=25°C; 1 h;
参考文献
Chang
Synthetic Communications, 1994 , vol. 24, # 7 p. 931 - 937
反应条件
1: 100 percent / sulfuric acid, iron / 0.5 h / 90 °C 2: 1.) 10percent aq. NaOH, 2.) sodium hydrosulfite / 1.) n-BuOH, 15 min, 2.) n-BuOH, 60 deg C, 30 min View Scheme
参考文献
Chang; Cheng
Synthetic Communications, 1995 , vol. 25, # 13 p. 1893 - 1900
反应条件
in nitrobenzene T=150°C; 7.5 h;
参考文献
DyStar Textilfarben GmbH and Co. Deutschland KG
Patent: US2010/64452 A1, 2010 ;
Location in patent: Page/Page column 5 ;
反应条件
sulfuric acid; iron T=90°C; 0.5 h;
参考文献
Chang; Cheng
Synthetic Communications, 1995 , vol. 25, # 13 p. 1893 - 1900
参考文献
Bayer and Co.
Patent: DE103395 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 5, p. 252