N-(4-氯-9,10-二氢-9,10-二氧代-1-蒽基)苯甲酰胺合成路线 (共 11 条)
反应条件
1: 76 percent / Copper powder / dimethylformamide / 1.5 h / Heating 2: conc.H2SO4 / 90 - 100 °C View Scheme
参考文献
Koshelev, V. I.; Paramonova, L. N.; Filippov, M. P.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 557 - 562
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 3 p. 622 - 628
反应条件
sodium carbonate; nitrobenzene; copper dichloride
参考文献
Du Pont de Nemours and Co.
Patent: US1884498 , 1929 ;
反应条件
sulfuric acid; boric acid T=140°C;
参考文献
German Dyestuffs and Dyestuff Intermediates
Fiat Final Report Nr. 1313, Bd. II <London 1948>, S. 200
反应条件
copper in N,N-dimethyl-formamide T=151 - 155°C; 1.5 h; Different solvents, diff.temp.,other conc. of Ia and Cu.; Product distribution;
参考文献
Koshelev, V. I.; Paramonova, L. N.; Filippov, M. P.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 557 - 562
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 3 p. 622 - 628
反应条件
anhydrous trichlorobenzene
Einleiten von Chlor in die verduennte oder mit Essigsaeure und Natriumacetat versetzte Reaktionsloesung bei 90-120grad;
参考文献
Du Pont de Nemours and Co.
Patent: US1963069 , 1931 ;
Full Text Show Details
Du Pont de Nemours and Co.
Patent: US1963109 , 1929 ;
参考文献
Mosgowa
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 773,774
Chem.Abstr., 1950 , p. 3480
反应条件
sulfuryl dichloride; nitrobenzene
参考文献
Gen. Aniline Works
Patent: US1772311 , 1927 ;
参考文献
Stanley; Adams
Journal of the American Chemical Society, 1931 , vol. 53, p. 2364,2367
参考文献
Bayer and Co.
Patent: DE228992 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 10, p. 644
反应条件
1: sodium acetate; copper (II)-acetate; copper (I)-chloride / weiteres Reagens: 1.2-Dichlor-benzol
2: sulfuric acid / anschliessend Behandeln mit Wasser
View Scheme
参考文献
Imp. Chem. Ind.
Patent: US1939218 , 1932 ;