反应条件
1: 1.) phosphorus oxychloride / 1.) 1,2-dichloroethane, reflux, 0.75 h, 2.) reflux, 1 h
2: 1.) NaH / 1.) DMF, RT, 1 h, 2.) 55 deg C, 5 h
3: 85percent m-chloroperbenzoic acid / CH2Cl2 / 3 h / 0 °C
4: 95 percent / HCl / 0.5 h / Heating
5: 1.) NaH / 1.) DMF, RT, 2.) 85 deg C, 5 h
View Scheme
参考文献
Franco, Fidencio; Greenhouse, Robert; Muchowski, Joseph M.
Journal of Organic Chemistry, 1982 , vol. 47, # 9 p. 1682 - 1688
