80937-33-3合成路线 （共 1249 条）
反应条件
in neat (no solvent) prepn. mechanochemically; FeS2 was activated using vibration mill; O2 atm.; steel reactor; time - 5 h; 20°C;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 53, # 7 p. 981 - 987
反应条件
in water prepn. mechanochemically; FeS2 was activated using vibration mill; O2 atm.; steel reactor; time - 5 h; 20°C;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 53, # 7 p. 981 - 987
反应条件
in melt under Ar in a tantalum ampoule, in Na melt, heating to 650 °C for7 d, oxygen as the contamination of SmI2; cooling in air to room temp., selected under a microscope;
参考文献
Ryazanov, Mikhail; Hoch, Constantin; Mattausch, Hansjuergen; Simon, Arndt
Zeitschrift fur Anorganische und Allgemeine Chemie, 2006 , vol. 632, # 15 p. 2385 - 2388
反应条件
in neat (no solvent) Irradiation (UV/VIS); photochemical react. of CS2-O2-mixtures on irradiation with light of a H2-discharge-tube, mechanism discussed;; main products SO2 and COS (spectroscopic identification), COS further oxidated;;
参考文献
Gmelin Handbook: S: MVol.B1, 88, page 194 - 196
反应条件
in neat (no solvent) byproducts: CO; slow, incomplete combustion of CS2, ratio O2:CS2 less than 2.5;; formation of SO2, CO and COS, smaller amounts of SO and CS obtained;;
参考文献
Gmelin Handbook: S: MVol.B1, 88, page 194 - 196
反应条件
in gaseous matrix Kinetics; Irradiation (UV/VIS); OH radical were generated by photolysis of H2O2; laser flash photolysisof OH and CS2 at 297+/-4 K; reaction mechanism discussed;; detn. by time-resolved tunable diode laser absorption spectroscopy;;
参考文献
Stickel, R. E.; Chin, M.; Daykin, E. P.; Hynes, A. J.; Wine, P. H.; Wallington, T. J.
Journal of Physical Chemistry, 1993 , vol. 97, # 51 p. 13653 - 13661
反应条件
byproducts: CO2; Irradiation (UV/VIS); 15 K, in solid O2; detd. by IR;
参考文献
Tso, Tai-Ly; Lee, Edward K. C.
Journal of Physical Chemistry, 1984 , vol. 88, # 13 p. 2781 - 2787
反应条件
sodium in neat (no solvent) reaction with detonation by redn. of VCl4 with Na;; >90percent, Cl-free V, purification respectively separation from V2O3 by treatment with HCl, formation of pyrophoric V powder after secondary treatment with H2 at red heat;;
参考文献
Roscoe, H. E.
Philosophical Transactions of the Royal Society of London, 1870 , vol. 160, p. 317 - 331
反应条件
in neat (no solvent) heating;;
参考文献
Morette, A.
Bull. Soc. Chim. Fr., Mem., 1942 , vol. 9, p. 146 - 152
Full Text Show Details
Morette, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1941 , vol. 212, p. 639 - 641
Full Text Show Details
Gmelin Handbook: V: MVol.B1, 141, page 364 - 367
反应条件
methylene blue; N-ethyl-N,N-diisopropylamine in water; acetonitrile T=20°C; 7 h; Schlenk techniqueIrradiation;
参考文献
Journal of the American Chemical Society, , vol. 135, # 36 p. 13286 - 13289
