6,6'-二硫烷二基二(1-己醇)合成路线 （共 5 条）
反应条件
1: pyridine / 4 h / 20 °C 2: 4-methyl-morpholine / dichloromethane / 0.33 h / 20 °C View Scheme
参考文献
Park, Jung Woo; Bang, Eun-Kyoung; Jeon, Eun Mi; Kim, Byeang Hyean
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 1 p. 96 - 102
参考文献
Renard, Brice-Loic; Lartia, Remy; Asseline, Ulysse
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 23 p. 4413 - 4425
反应条件
iodine; triethylamine in methanol
T=0 - 20°C; 4 h;
参考文献
Park, Jung Woo; Bang, Eun-Kyoung; Jeon, Eun Mi; Kim, Byeang Hyean
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 1 p. 96 - 102
反应条件
[BnEt3N]2MoS4 in acetonitrile
T=25°C; 15 h;
参考文献
Prabhu, Kandikere R.; Ramesha, A. R.; Chandrasekaran, Srinivasan
Journal of Organic Chemistry, 1995 , vol. 60, # 22 p. 7142 - 7143
反应条件
1.1: thiourea / ethanol / Heating; Inert atmosphere
1.2: Inert atmosphere
2.1: iodine / ethanol / 20 °C / Inert atmosphere
View Scheme
参考文献
Luska, Kylie L.; Moores, Audrey
Canadian Journal of Chemistry, 2012 , vol. 90, # 1 p. 145 - 152
