2-乙酰氨基-3-O-苄基-4,6-O-亚苄基-2-脱氧-β-D-半乳糖-1-叠氮化物合成路线 （共 3 条）
反应条件
Ba(OH)2*8H2O; BaO in N,N-dimethyl-formamide
2 h; Ambient temperature1.) N,N-dimethylformamide, RT, 2 h, 2.) chloroform, reflux, 2 h;
参考文献
Shaban, Mohammed Abd El-Monem; Jeanloz, Roger W.
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 11 p. 3570 - 3576
反应条件
1: 76 percent / formic acid / 0.5 h / Ambient temperature
2: 82 percent / barium oxide, barium hydroxide octahydrate / dimethylformamide / 2 h / Ambient temperature; 1.) N,N-dimethylformamide, RT, 2 h, 2.) chloroform, reflux, 2 h
View Scheme
参考文献
Shaban, Mohammed Abd El-Monem; Jeanloz, Roger W.
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 11 p. 3570 - 3576
反应条件
1: 76 percent / formic acid / 0.5 h / Ambient temperature
2: 82 percent / barium oxide, barium hydroxide octahydrate / dimethylformamide / 2 h / Ambient temperature; 1.) N,N-dimethylformamide, RT, 2 h, 2.) chloroform, reflux, 2 h
View Scheme
参考文献
Shaban, Mohammed Abd El-Monem; Jeanloz, Roger W.
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 11 p. 3570 - 3576
