2,3-二甲基-4-硝基苯胺合成路线 （共 16 条）
反应条件
1: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, aq. CuSO4 2: H2SO4 3: H2SO4, aq. NaNO2 4: H2SO4 / Heating 5: SnCl2, aq. HCl, AcOH 6: aq. NaNO2, aq. H2SO4 7: aq. NaOH 8: aq. NaOH View Scheme
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
反应条件
1: (i) NaNO2, aq. HCl, (ii) /BRN= 4652394/, aq. CuSO4 2: H2SO4 3: H2SO4, aq. NaNO2 4: aq. NH3, aq. FeSO4 / Heating View Scheme
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
反应条件
sulfuric acid; sodium nitrite anschliessend Behandeln mit wss. Hypophosphorigsaeure;
参考文献
van Helden et al.
Recueil des Travaux Chimiques des Pays-Bas, 1954 , vol. 73, p. 39,47
反应条件
acetic acid; sodium nitrite Diazotization;
参考文献
Noelting
Chemische Berichte, 1904 , vol. 37, p. 2583
反应条件
sulfuric acid in water
1 h; Heating / reflux;
参考文献
Bayer Corporation
Patent: US6353006 B1, 2002 ;
Location in patent: Page column 28-29 ;
US 6353006 B1
反应条件
sulfuric acid
1 h; Heating;
参考文献
Kanetani, Fujio; Yamaguchi, Hachiro
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # l0 p. 3048 - 3058
反应条件
sulfuric acid; nitric acid
T=0°C; 1 h;
参考文献
Havlik, Martin; Kral, Vladimir; Kaplanek, Robert; Dolensky, Bohumil
Organic Letters, 2008 , vol. 10, # 21 p. 4767 - 4769
反应条件
sulfuric acid; nitric acid
参考文献
Vene,J. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 1813 - 1817
参考文献
Noelting; Braun; Thesmar
Chemische Berichte, 1901 , vol. 34, p. 2255
反应条件
1: 1.) NaNO2, HCl, 2.) SO2, CuCl2
2: Na2CO3 / methanol / 1 h / Heating
3: Fe
View Scheme
参考文献
Kanetani, Fujio; Yamaguchi, Hachiro
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # l0 p. 3048 - 3058
