2,3,6,7,10,11-六甲氧基三亚苯合成路线 （共 19 条）
反应条件
in acetonitrile electrochemically: platinum sheet, glassy carbon rod; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 32, # 50 p. 7405 - 7408
反应条件
tetra-n-butylammonium tetrafluoroborate; triethylamine 1.) acetonitrile, anodic oxidation, 2.) acetonitrile or pentane, Et3N, room temperature, 2 h; Multistep reaction;
参考文献
Tetrahedron, , vol. 47, # 4/5 p. 791 - 798
反应条件
tetra-n-butylammonium tetrafluoroborate; triethylamine 1.) acetonitrile, anodic oxidation, 2.) acetonitrile or pentane, Et3N, room temperature, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 47, # 4/5 p. 791 - 798
反应条件
in acetonitrile anodic oxidation; other substrates;
参考文献
Tetrahedron, , vol. 47, # 4/5 p. 791 - 798
反应条件
boron tribromide in dichloromethane T=-70 - 20°C;
参考文献
Zniber, Rachid; Achour, Redouane; Cherkaoui, Mohammed Zoubair; Donnio, Bertrand; Gehringer, Lionel; Guillon, Daniel
Journal of Materials Chemistry, 2002 , vol. 12, # 8 p. 2208 - 2213
反应条件
sulfuric acid; boron tribromide 1.) anhydr. CH2Cl2, 4 h; 2.) reflux, 30 min; Yield given. Multistep reaction;
参考文献
Naarmann; Hanack; Mattmer
Synthesis, 1994 , vol. 1, # 5 p. 477 - 478
反应条件
1: CHCl3 / Heating
2: 54 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 80 °C
View Scheme
参考文献
Chiang, Long Y.; Safinya, C. R.; Clark, N. A.; Liang, K. S.; Bloch, A. N.
Journal of the Chemical Society, Chemical Communications, 1985 , # 11 p. 695 - 696
反应条件
1: CHCl3 / Heating
2: 54 percent / TBAF / tetrahydrofuran / 80 °C
View Scheme
参考文献
Chiang, Long Y.; Safinya, C. R.; Clark, N. A.; Liang, K. S.; Bloch, A. N.
Journal of the Chemical Society, Chemical Communications, 1985 , # 11 p. 695 - 696
反应条件
1: CHCl3 / Heating
2: 54 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 80 °C
View Scheme
参考文献
Chiang, Long Y.; Stokes, James P.; Safinya, Cyrus R.; Bloch, Aaron N.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 125, p. 279 - 288
