2,3,6,7,10,11-六甲氧基三亚苯合成路线 (共 19 条)
反应条件
anhydrous iron chloride in dichloromethane
参考文献
Wei, Junfa; Han, Bo; Guo, Qiang; Shi, Xianying; Wang, Wenliang; Wei, Ni
Angewandte Chemie - International Edition, 2010 , vol. 49, # 44 p. 8209 - 8213
反应条件
iron(III) chloride in dichloromethane 12 h; Ambient temperature;
参考文献
McKillop, Alexander; Turrell, Andrew G.; Young, Derek W.; Taylor, Edward C.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6504 - 6512
反应条件
tetra-n-butylammonium tetrafluoroborate in dichloromethane; trifluoroacetic acid T=12°C; electrolysis, other solvent; Further byproducts given;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 36, # 5 p. 317 - 326
反应条件
iron(III) chloride; 3,3',4,4'-tetrakis(n-hexyloxy)biphenyl in dichloromethane 1 h; Ambient temperature;
参考文献
Boden, Neville; Bushby, Richard J.; Cammidge, Andrew N.
Journal of the Chemical Society, Chemical Communications, 1994 , # 4 p. 465 - 466
反应条件
tetra-n-butylammonium tetrafluoroborate in dichloromethane; trifluoroacetic acid T=12°C; electrolysis, other solvent; Further byproducts given;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 36, # 5 p. 317 - 326
反应条件
iron(III) chloride in dichloromethane 1 h; Ambient temperature;
参考文献
Boden, Neville; Bushby, Richard J.; Cammidge, Andrew N.
Journal of the Chemical Society, Chemical Communications, 1994 , # 4 p. 465 - 466
反应条件
1.1: isopropylmagnesium chloride / diethyl ether; tetrahydrofuran / 2 h / -78 °C 1.2: 20 °C 1.3: 0.5 h / 20 °C 2.1: diethyl ether / 20 °C 3.1: bis(dibenzylideneacetone)-palladium(0); bis[2-(diphenylphosphino)phenyl] ether; potassium tert-butylate / toluene / 100 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 16, # 9 p. 2338 - 2341
反应条件
benzo-15-crown-5 in acetonitrile electrochemically: platinum sheet, glassy carbon rod; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 32, # 50 p. 7405 - 7408
反应条件
in acetonitrile electrochemically: platinum sheet, glassy carbon rod; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 32, # 50 p. 7405 - 7408
反应条件
in acetonitrile electrochemically: platinum sheet, glassy carbon rod; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 32, # 50 p. 7405 - 7408