二氯(1-甲基乙基)-镁酸锂盐合成路线 (共 11 条)
反应条件
1: 6-Methoxyquinoline With boron trifluoride diethyl etherate in tetrahydrofuran
T=0°C; 0.25 h; Inert atmosphere;
2: isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran
T=-50°C; 0.5 h; Inert atmosphere;
3: With chloranil in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere; regioselective reaction;
参考文献
Chen, Quan; Du Jourdin, Xavier Mollat; Knochel, Paul
Journal of the American Chemical Society, 2013 , vol. 135, # 13 p. 4958 - 4961