alpha-(三氯甲基)-2-吡啶甲醇合成路线 (共 5 条)
反应条件
malonic acid in dimethyl sulfoxide
T=20°C; 0.666667 h;
参考文献
Jensen, Andreas B.; Lindhardt, Anders T.
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1174 - 1183
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene
T=20°C; 12 h;
参考文献
Ram, Ram N.; Manoj
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5633 - 5635
反应条件
hydrogenchloride in methanol
3 h; Heating; Yield given;
参考文献
Deleris; Dunogues; Babin; et al.
European Journal of Medicinal Chemistry, 1981 , vol. 16, # 6 p. 533 - 537
反应条件
1: 21 h / 90 - 100 °C
2: conc. HCl / methanol / 3 h / Heating
View Scheme
参考文献
Deleris; Dunogues; Babin; et al.
European Journal of Medicinal Chemistry, 1981 , vol. 16, # 6 p. 533 - 537
反应条件
[2,2']bipyridinyl; copper(l) chloride in 1,2-dichloro-ethane
3 h; Heating;
参考文献
Ram, Ram N.; Manoj
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5633 - 5635