反应条件
1: 1) 1.98 M BuLi / 1) n-hexane, THF, -78 to 0 deg C, 2) THF, 30 min, 25 deg C
2: NCS, AgNO3 / acetonitrile / 15 h / 40 - 50 °C
3: LiAlH4 / diethyl ether / 3 h / 35 °C
4: NEt3 / CH2Cl2 / 4 h / 25 °C
5: dimethylformamide / 6 h / 120 °C
View Scheme
参考文献
Kaulen, Johannes
Angewandte Chemie, 1989 , vol. 101, # 4 p. 507 - 508
