5-氨基-3-beta-D-呋喃核糖基咪唑并(4,5-d)(1,3)恶嗪-7(3H)-酮合成路线 （共 16 条）
反应条件
hydrogen; palladium on activated charcoal in N,N-dimethyl-formamide
参考文献
Luk, Kin-Chun; Moore, Douglas W.; Keith, Dennis D.
Tetrahedron Letters, 1994 , vol. 35, # 7 p. 1007 - 1010
反应条件
1-(3-dimethylaminopropyl)-3-ethylcarbodiinide hydrochloride in methanol; water
参考文献
Luk, Kin-Chun; Moore, Douglas W.; Keith, Dennis D.
Tetrahedron Letters, 1994 , vol. 35, # 7 p. 1007 - 1010
反应条件
1: 48 percent / nBu4NI, K2CO3 / dimethylformamide
2: 1,2-dichloro-ethane
3: 44 percent / NH3 / methanol
4: 75 percent / H2 / 10percent Pd/C / ethanol
5: 89 percent / (CH3)2N(CH2)3NCNC2H5*HCl / methanol; H2O
View Scheme
参考文献
Luk, Kin-Chun; Moore, Douglas W.; Keith, Dennis D.
Tetrahedron Letters, 1994 , vol. 35, # 7 p. 1007 - 1010
反应条件
1: 1,2-dichloroethane
2: KOH / methanol
3: 73 percent / H2 / 10percent Pd/C / dimethylformamide
4: 89 percent / (CH3)2N(CH2)3NCNC2H5*HCl / methanol; H2O
View Scheme
参考文献
Luk, Kin-Chun; Moore, Douglas W.; Keith, Dennis D.
Tetrahedron Letters, 1994 , vol. 35, # 7 p. 1007 - 1010
反应条件
1: 73 percent / H2 / 10percent Pd/C / dimethylformamide
2: 89 percent / (CH3)2N(CH2)3NCNC2H5*HCl / methanol; H2O
View Scheme
参考文献
Luk, Kin-Chun; Moore, Douglas W.; Keith, Dennis D.
Tetrahedron Letters, 1994 , vol. 35, # 7 p. 1007 - 1010
反应条件
1: KOH / methanol
2: 73 percent / H2 / 10percent Pd/C / dimethylformamide
3: 89 percent / (CH3)2N(CH2)3NCNC2H5*HCl / methanol; H2O
View Scheme
参考文献
Luk, Kin-Chun; Moore, Douglas W.; Keith, Dennis D.
Tetrahedron Letters, 1994 , vol. 35, # 7 p. 1007 - 1010
反应条件
1: DCC / dimethylformamide
2: 75 percent / H2 / 10percent Pd/C / dimethylformamide
View Scheme
参考文献
Luk, Kin-Chun; Moore, Douglas W.; Keith, Dennis D.
Tetrahedron Letters, 1994 , vol. 35, # 7 p. 1007 - 1010
反应条件
1: 75 percent / H2 / 10percent Pd/C / ethanol
2: 89 percent / (CH3)2N(CH2)3NCNC2H5*HCl / methanol; H2O
View Scheme
参考文献
Luk, Kin-Chun; Moore, Douglas W.; Keith, Dennis D.
Tetrahedron Letters, 1994 , vol. 35, # 7 p. 1007 - 1010
反应条件
1: 1,2-dichloro-ethane
2: 44 percent / NH3 / methanol
3: 75 percent / H2 / 10percent Pd/C / ethanol
4: 89 percent / (CH3)2N(CH2)3NCNC2H5*HCl / methanol; H2O
View Scheme
参考文献
Luk, Kin-Chun; Moore, Douglas W.; Keith, Dennis D.
Tetrahedron Letters, 1994 , vol. 35, # 7 p. 1007 - 1010
反应条件
in water
2 h; Ambient temperatureIrradiation;
参考文献
De Napoli, Lorenzo; Di Fabio, Giovanni; Messere, Anna; Montesarchio, Daniela; Piccialli, Gennaro; Varra, Michela
Tetrahedron Letters, 1998 , vol. 39, # 40 p. 7397 - 7400
